13C-detected 1H–2H separated local field NMR spectroscopy

Dvinskikh, Sergey V.; Sandström, Dick; Zimmermann, Herbert; Maliniak, Arnold

doi:10.1016/j.cplett.2003.10.071

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13C-detected 1H–2H separated local field NMR spectroscopy

Dvinskikh, S. V., Sandström, D., Zimmermann, H., & Maliniak, A. (2003). 13C-detected 1H–2H separated local field NMR spectroscopy. Chemical Physics Letters, 382(3), 410-417. doi:10.1016/j.cplett.2003.10.071.

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Item Permalink: https://hdl.handle.net/21.11116/0000-0000-3B1E-E Version Permalink: https://hdl.handle.net/21.11116/0000-0000-3B1F-D

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Dvinskikh, Sergey V., Author
Sandström, Dick, Author
Zimmermann, Herbert^{1, 2, 3, 4}, Author
Maliniak, Arnold, Author

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1Department of Molecular Physics, Max Planck Institute for Medical Research, Max Planck Society, ou_1497705
2Department of Biomolecular Mechanisms, Max Planck Institute for Medical Research, Max Planck Society, ou_1497700
3Zimmermann Group, Max Planck Institute for Medical Research, Max Planck Society, ou_1497749
4Emeritus Group Biophysics, Max Planck Institute for Medical Research, Max Planck Society, ou_1497712

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Abstract: We present a new NMR method for measuring 1H–2H dipolar couplings in macroscopically oriented media. To overcome the lack of dipolar resolution in 1D 1H and 2H spectra of deuterated molecules, we use a 2D heteronuclear correlation experiment where 1H chemical shifts and 1H–2H dipolar interactions in the first dimension are correlated with 13C chemical shifts and 2H–13C dipolar interactions in the second dimension. The technique is demonstrated on a columnar liquid-crystalline phase.

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Language(s): eng - English

Dates: Submitted: 2003-09-08Accepted: 2003-10-17Date issued: 2003-12-05

Publication Status: Issued

Pages: 8

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Identifiers: DOI: 10.1016/j.cplett.2003.10.071

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Title: Chemical Physics Letters

Alternative Title : Chem. Phys. Lett.

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Pages: - Volume / Issue: 382 (3) Sequence Number: - Start / End Page: 410 - 417 Identifier: -