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  Application of phase correction to improve the characterization of photooxidation products of lignin using 7 Tesla Fourier-transform ion cyclotron resonance mass spectrometry

Qi, Y., Luo, R., Schrader, W., & Volmer, D. A. (2017). Application of phase correction to improve the characterization of photooxidation products of lignin using 7 Tesla Fourier-transform ion cyclotron resonance mass spectrometry. FACETS, 2, 461-475. doi:10.1139/facets-2016-0069.

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 Creators:
Qi, Yulin1, Author
Luo, Ruoji2, Author           
Schrader, Wolfgang2, Author           
Volmer, Dietrich A.1, Author
Affiliations:
1Institute of Bioanalytical Chemistry, Saarland University, D-66123 Saarbrücken, Germany, ou_persistent22              
2Service Department Schrader (MS), Max-Planck-Institut für Kohlenforschung, Max Planck Society, ou_1445629              

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 Abstract: Lignin is the second most abundant natural biopolymer and potentially a valuable alternative energy source for conventional fossil fuels. In this study, Fourier-transform ion cyclotron resonance-mass spectrometry (FTICR-MS) in conjunction with phase correction was applied to study photooxidation products of lignin using a 7 Tesla (T) mass spectrometer. The application of 7 T FTICR-MS has often been inadequate for the analysis of complex natural organic matter because of insufficient resolving power as compared with high-field FTICR, which led to incorrect assignments of elemental formulae and discontinuous plots in graphical and statistical analyses. Here, the application of phase correction to the FTICR mass spectra of lignin oxidation products greatly improved the spectral quality, and thus, readily permitted characterization of photooxidation processes of lignin compounds under simulated solar radiation conditions.

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Language(s): eng - English
 Dates: 2016-11-242017-04-192017-05-30
 Publication Status: Published online
 Pages: 15
 Publishing info: -
 Table of Contents: -
 Rev. Type: Peer
 Identifiers: DOI: 10.1139/facets-2016-0069
 Degree: -

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Title: FACETS
Source Genre: Journal
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Publ. Info: Ottawa; Kanada : Canadian Science Publishing
Pages: - Volume / Issue: 2 Sequence Number: - Start / End Page: 461 - 475 Identifier: ISSN: 2371-1671
CoNE: https://pure.mpg.de/cone/journals/resource/2371-1671