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  Simple vapor-solid synthesis of Zn-based intermetallic compounds

Ivarsson, D. C. A., Burkhardt, U., Richter, K. W., Kriegel, R., Rossner, L., Neumann, M., et al. (2018). Simple vapor-solid synthesis of Zn-based intermetallic compounds. Journal of Alloys and Compounds, 743, 155-162. doi:10.1016/j.jallcom.2018.01.385.

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Item Permalink: http://hdl.handle.net/21.11116/0000-0001-2286-1 Version Permalink: http://hdl.handle.net/21.11116/0000-0001-2636-8
Genre: Journal Article

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 Creators:
Ivarsson, Dennis C. A.1, Author
Burkhardt, Ulrich2, Author              
Richter, Klaus W.1, Author
Kriegel, René1, Author
Rossner, Leonard1, Author
Neumann, Matthias3, Author              
Armbrüster, Marc1, Author
Affiliations:
1External Organizations, ou_persistent22              
2Ulrich Burkhardt, Chemical Metal Science, Max Planck Institute for Chemical Physics of Solids, Max Planck Society, ou_1863422              
3Chemical Metal Science, Max Planck Institute for Chemical Physics of Solids, Max Planck Society, ou_1863405              

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 Abstract: A synthesis route to ZnPd, ZnPt and Cu5Zn8 based on a vapor-solid reaction of stoichiometric amounts of the elements is presented. The high vapor pressure of zinc, usually hindering a controlled synthesis, forms part of the developed synthesis strategy with a focus on the catalytically active intermetallic compound ZnPd. The method provides excellent compositional control of better than 0.1 at% and results in dense samples without requiring detailed knowledge of the corresponding thermodynamics. Utilizing the well-defined ZnPd samples, the bulk defect model as well as the reducibility of surface oxides was clarified. The well-controlled synthesis route creates new opportunities for exploring the reaction kinetics and formation processes of intermetallic compounds. (c) 2018 Elsevier B.V. All rights reserved.

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Language(s): eng - English
 Dates: 2018-02-022018-02-02
 Publication Status: Published in print
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 Table of Contents: -
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Title: Journal of Alloys and Compounds
  Abbreviation : J. Alloy. Comp.
Source Genre: Journal
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Publ. Info: Lausanne, Switzerland : Elsevier B.V.
Pages: - Volume / Issue: 743 Sequence Number: - Start / End Page: 155 - 162 Identifier: ISSN: 0925-8388
CoNE: https://pure.mpg.de/cone/journals/resource/954925567746