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  Identification of polymer matrix yield stress in the wood cell wall based on micropillar compression and micromechanical modelling

Schwiedrzik, J., Raghavan, R., Rüggeberg, M., Hansen, S., Wehrs, J., Adusumalli, R. B., et al. (2016). Identification of polymer matrix yield stress in the wood cell wall based on micropillar compression and micromechanical modelling. Philosophical Magazine, 96(32-34), 3461-3478. doi:10.1080/14786435.2016.1235292.

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Schwiedrzik, Jakob1, Autor           
Raghavan, Rejin2, 3, Autor           
Rüggeberg, Markus4, 5, Autor           
Hansen, Silla1, 6, Autor           
Wehrs, Juri2, Autor           
Adusumalli, Ramesh B.1, 7, Autor           
Zimmermann, Tanja5, Autor           
Michler, Johann8, Autor           
Affiliations:
1Laboratory for Mechanics of Materials and Nanostructures, Empa Swiss Federal Laboratories for Material Science and Technology, Thun, Switzerland, persistent22              
2Empa, Swiss Federal Laboratories for Materials Science and Technology, Laboratory for Mechanics of Materials and Nanostructures, Feuerwerkerstrasse 39, Thun, Switzerland, ou_persistent22              
3Synthesis of Nanostructured Materials, Structure and Nano-/ Micromechanics of Materials, Max-Planck-Institut für Eisenforschung GmbH, Max Planck Society, ou_1863403              
4Institute for Building Materials, ETH Zürich, Zürich, Switzerland, persistent22              
5Laboratory for Applied Wood Materials, Empa Swiss Federal Laboratories for Materials Science and Technology, Dübendorf, Switzerland, persistent22              
6Institute for Biological Interfaces, Karlsruhe Institute of Technology, Eggenstein-Leopoldshafen, Germany, persistent22              
7Department of Chemical Engineering, BITS Pilani-Hyderabad Campus, Hyderabad, India, persistent22              
8Empa – Swiss Federal Laboratories for Materials Science and Technology, Laboratory for Mechanics of Materials and Nanostructures, Thun, Switzerland, persistent22              

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Schlagwörter: Biomechanics; Cells; Composite micromechanics; Cytology; Lignin; Micromechanics; Polymer matrix; Stresses; Wood, Continuum micromechanics; Experimental approaches; Hierarchical materials; Inhomogeneous materials; Micro-mechanical modeling; Micro-pillar compressions; Micromechanical modelling; Wood cell walls, Yield stress
 Zusammenfassung: Based on a combination of micropillar compression experiments and modelling of the secondary cell wall (cw) using continuum micromechanics, the shear yield stress of the polymer matrix is identified for both normal and compression wood of Norway spruce. It is shown that the model is able to capture the differences in mechanical properties between the two tissues based on the knowledge of composition of the samples, microfibril angle, as well as phase properties on the nanometer scale. By testing an isolated piece of the cell wall with a homogeneous and uniaxial stress field on the micrometer scale and using the micromechanical model to determine average stress fields on the nanometer scale, it is possible to identify the shear yield stress of the polymer matrix in wood, which was found to be in the range of 14.9–17.5 MPa for normal and compression wood. It was shown that this corresponds to a stress in the lignin phase of approx. 17 MPa. This combined study thus demonstrates a new approach for validating multiscale models predicting yield properties with uniaxial experiments at the microscale and measuring phase properties of inhomogeneous materials by a combination of modelling and experimental approaches. © 2016 Empa Swiss Federal Laboratory for Materials Science and Technology.

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Sprache(n): eng - English
 Datum: 2016-12-01
 Publikationsstatus: Erschienen
 Seiten: -
 Ort, Verlag, Ausgabe: -
 Inhaltsverzeichnis: -
 Art der Begutachtung: Expertenbegutachtung
 Identifikatoren: DOI: 10.1080/14786435.2016.1235292
BibTex Citekey: Schwiedrzik20163461
 Art des Abschluß: -

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Titel: Philosophical Magazine
  Kurztitel : Philos. Mag.
Genre der Quelle: Zeitschrift
 Urheber:
Affiliations:
Ort, Verlag, Ausgabe: Milton Park, Abingdon, England : Taylor & Francis
Seiten: - Band / Heft: 96 (32-34) Artikelnummer: - Start- / Endseite: 3461 - 3478 Identifikator: ISSN: 1478-6435
CoNE: https://pure.mpg.de/cone/journals/resource/954925265237