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  Sonochemical preparation of silane-coated titania particles

Shafi, K. V. P. M., Ulman, A., Yan, X., Yang, N.-L., Himmelhaus, M., & Grunze, M. (2001). Sonochemical preparation of silane-coated titania particles. Langmuir, 17(5), 1726-1730. doi:10.1021/la001252g.

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Item Permalink: https://hdl.handle.net/21.11116/0000-0001-BDE9-4 Version Permalink: https://hdl.handle.net/21.11116/0000-0001-BDEA-3
Genre: Journal Article

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Langmuir_17_2001_1726.pdf (Any fulltext), 123KB
 
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 Creators:
Shafi, Kurikka V. P. M., Author
Ulman, Abraham, Author
Yan, Xingzhong, Author
Yang, Nan-Loh, Author
Himmelhaus, Michael, Author
Grunze, Michael1, Author           
Affiliations:
1Cellular Biophysics, Max Planck Institute for Medical Research, Max Planck Society, ou_2364731              

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 Abstract: We report that sonochemistry is a fast and efficient technique for coating of octadecyltrihydrosilane (CH3(CH2)17SiH3) on titania surfaces. Infrared spectroscopy as well as thermal analysis confirms that complete coating is achieved after 30 min. Solid-state 13C NMR spectroscopy establishes the bonding of trihydrosilane to the titania particles. Raman microscopy gives the expected rutile structure and further confirms the presence of an octadecyl monolayer. X-ray diffraction confirms that the rutile structure of the titania particles has not changed during sonication. Anatase titania undergoes the same reaction when sonicated in the presence of octadecyltrihydrosilane.

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Language(s): eng - English
 Dates: 2000-12-212000-08-302001-02-012001
 Publication Status: Issued
 Pages: 5
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 Table of Contents: -
 Rev. Type: Peer
 Identifiers: DOI: 10.1021/la001252g
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Title: Langmuir
Source Genre: Journal
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Publ. Info: Columbus, OH : American Chemical Society
Pages: - Volume / Issue: 17 (5) Sequence Number: - Start / End Page: 1726 - 1730 Identifier: ISSN: 0743-7463
CoNE: https://pure.mpg.de/cone/journals/resource/954925541194