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  A comparative study of electrochemical cells for in situ X-ray spectroscopies in the soft and tender X-ray range

Velasco Vélez, J., Falling, L., Bernsmeier, D., Sear, M. J., Clark, P. C. J., Chan, T. S., et al. (2021). A comparative study of electrochemical cells for in situ X-ray spectroscopies in the soft and tender X-ray range. Journal of Physics D, 54(12): 124003. doi:10.1088/1361-6463/abd2ed.

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Velasco+Vélez+et+al_2020_J._Phys._D _Appl._Phys._10.1088_1361-6463_abd2ed.pdf (Any fulltext), 15MB
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Velasco+Vélez+et+al_2020_J._Phys._D _Appl._Phys._10.1088_1361-6463_abd2ed.pdf
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2020
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Velasco Vélez, Juan1, Author           
Falling, Lorenz1, Author           
Bernsmeier, Dennis2, Author
Sear, Michael J.3, Author
Clark, Pip C J3, Author
Chan, Ting Shan4, Author
Stotz, Eugen1, Author           
Hävecker, Michael1, Author           
Kraehnert, Ralph2, Author
Knop-Gericke, Axel1, Author           
Chuang, Cheng-Hao Chuang5, Author
Starr, David E.3, Author
Favaro, Marco3, Author
Mom, Rik6, Author
Affiliations:
1Inorganic Chemistry, Fritz Haber Institute, Max Planck Society, ou_24023              
2Institut für Chemie, TU Berlin, Berlin, Berlin, GERMANY, ou_persistent22              
3Institute of Solar Fuels, Helmholtz-Zentrum Berlin fur Materialien und Energie GmbH, Berlin, Berlin, GERMANY, ou_persistent22              
4National Synchrotron Radiation Research Centre, Hsinchu, TAIWAN, ou_persistent22              
5Tamkang University, Taipei, TAIWAN, ou_persistent22              
6Leiden Institute of Chemistry, Leiden University, Leiden, 2300 RA, NETHERLANDS, ou_persistent22              

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 Abstract: In situ X-ray spectroscopies offer a powerful way to understand the electronic structure of the electrode-electrolyte interface under operating conditions. However, most X-ray techniques require vacuum, making it necessary to design spectro-electrochemical cells with a delicate interface to the wet electrochemical environment. The design of the cell often dictates what measurements can be done and which electrochemical processes can be studied. Hence, it is important to pick the right spectro-electrochemical cell for the process of interest. To facilitate this choice, and to highlight the challenges in cell design, we critically review four recent, successful cell designs. Using several case studies, we investigate the opportunities and limitations that arise in practical experiments.

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Language(s): eng - English
 Dates: 2020-10-302020-12-112020-12-112021-03-25
 Publication Status: Published in print
 Pages: 14
 Publishing info: -
 Table of Contents: -
 Rev. Type: Peer
 Identifiers: DOI: 10.1088/1361-6463/abd2ed
 Degree: -

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Title: Journal of Physics D
  Abbreviation : J. Phys. D: Appl. Phys.
Source Genre: Journal
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Publ. Info: Bristol : IOP Publishing
Pages: 14 Volume / Issue: 54 (12) Sequence Number: 124003 Start / End Page: - Identifier: ISSN: 0022-3727
CoNE: https://pure.mpg.de/cone/journals/resource/0022-3727