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  Vacuum compatible flow-cell for high-quality in situ and operando soft X-ray photon-in–photon-out spectroelectrochemical studies of energy materials

Tesch, M. F., Bonke, S. A., Golnak, R., Xiao, J., Simonov, A. N., & Schlögl, R. (2022). Vacuum compatible flow-cell for high-quality in situ and operando soft X-ray photon-in–photon-out spectroelectrochemical studies of energy materials. Electrochemical Science Advances, 2(6): e2100141. doi:10.1002/elsa.202100141.

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Item Permalink: https://hdl.handle.net/21.11116/0000-0009-B62A-B Version Permalink: https://hdl.handle.net/21.11116/0000-000C-45AE-3
Genre: Journal Article

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Electrochemical Science Adv - 2021 - Tesch - Vacuum compatible flow‐cell for high‐quality in situ and operando soft X‐ray.pdf (Publisher version), 2MB
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Electrochemical Science Adv - 2021 - Tesch - Vacuum compatible flow‐cell for high‐quality in situ and operando soft X‐ray.pdf
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2022
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 Creators:
Tesch, Marc F.1, Author
Bonke, Shannon A.2, Author
Golnak, Ronny3, Author
Xiao, Jie3, Author
Simonov, Alexandr N.4, Author
Schlögl, Robert1, 5, Author           
Affiliations:
1Department Heterogeneous Reactions, Max Planck Institute for Chemical Energy Conversion, Mülheim an der Ruhr, Germany, ou_persistent22              
2Yusuf Hamied Department of Chemistry, University of Cambridge, Cambridge, UK, ou_persistent22              
3Department of Highly Sensitive X-ray Spectroscopy, Helmholtz-Zentrum Berlin für Materialien und Energie GmbH, Berlin, Germany, ou_persistent22              
4School of Chemistry and the ARC Centre of Excellence for Electromaterials Science, Monash University, Victoria 3800, Australia, ou_persistent22              
5Inorganic Chemistry, Fritz Haber Institute, Max Planck Society, ou_24023              

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 Abstract: Soft X-ray spectroscopy is a powerful method to investigate materials on anelement selective level with respect to their atomic and electronic structure.However, its application is technically challenging for in situ oroperandoinvestigations of materials for electrochemical applications. Herein, we presenta spectroelectrochemical flow-cell designed to enable state-of-the-art elec-trochemical characterization while being installed in a vacuum chamber forthe direct accessibility of the electroactive sample to soft X-rays. An overviewof the application of soft X-ray photon-in–photon-out spectroscopic studiesto electromaterials is provided, along with discussions of experimental andtechnical considerations specific to this highly sensitive mode of analysis.Application of the cell for the in situ spectroelectrochemical characterization ofan electrodeposited nickel oxide water electrooxidation catalyst is demonstrated.

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Language(s): eng - English
 Dates: 2021-07-312021-11-292022-12
 Publication Status: Published online
 Pages: 10
 Publishing info: -
 Table of Contents: -
 Rev. Type: Peer
 Identifiers: DOI: 10.1002/elsa.202100141
 Degree: -

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Title: Electrochemical Science Advances
  Other : ELSA
  Abbreviation : Electrochem. Sci. Adv.
Source Genre: Journal
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Publ. Info: Weinheim : Wiley-VCH
Pages: 10 Volume / Issue: 2 (6) Sequence Number: e2100141 Start / End Page: - Identifier: ISSN: 2698-5977
CoNE: https://pure.mpg.de/cone/journals/resource/2698-5977