Structure elucidation of the core octasaccharide from Citrobacter PCM 1487 with 
the aid of 500-MHz, two-dimensional phase-sensitive correlated, 
relayed-coherence transfer, double-quantum, triple-quantum filtered, and N.O.E. 
1H-n.m.r. spectra

Dabrowski, Janusz; Hauck, Michael; Romanowska, Elzbieta; Gamian, Andrzej

doi:10.1016/0008-6215(88)80074-0

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Structure elucidation of the core octasaccharide from Citrobacter PCM 1487 with the aid of 500-MHz, two-dimensional phase-sensitive correlated, relayed-coherence transfer, double-quantum, triple-quantum filtered, and N.O.E. 1H-n.m.r. spectra

Dabrowski, J., Hauck, M., Romanowska, E., & Gamian, A. (1988). Structure elucidation of the core octasaccharide from Citrobacter PCM 1487 with the aid of 500-MHz, two-dimensional phase-sensitive correlated, relayed-coherence transfer, double-quantum, triple-quantum filtered, and N.O.E. 1H-n.m.r. spectra. Carbohydrate Research, 180(2), 163-174. doi:10.1016/0008-6215(88)80074-0.

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Item Permalink: https://hdl.handle.net/21.11116/0000-000A-54E9-1 Version Permalink: https://hdl.handle.net/21.11116/0000-000A-54EA-0

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https://www.sciencedirect.com/science/article/pii/0008621588800740/pdf?md5=cd3f7751ee54c84c5e4b7d177e161db7&pid=1-s2.0-0008621588800740-main.pdf (Any fulltext) Open Access status unknown

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Creators:
Dabrowski, Janusz¹, Author
Hauck, Michael¹, Author
Romanowska, Elzbieta, Author
Gamian, Andrzej, Author

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1Department of Organic Chemistry, Max Planck Institute for Medical Research, Max Planck Society, ou_1497706

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Abstract: The main features of the primary structure of the octasaccharide, α-d-Glcp-(1→2)-α-d-Glcp-(1→2)-[α-d-GalpNAc- (1→3)]-α-d-Galp-(1→3)-α-d-Glcp-(1→3)-[α-ld-Hepp-(1→7)]-α-ld-Hepp-(1→3)-α-ld-Hep, have been determined in the ab initio manner by 1H-n.m.r. spectroscopy without resorting to biochemical methods of analysis. Several nontypical interresidue n.O.e. values point to a preferred solution conformation of the molecule.

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Language(s): eng - English

Dates: Submitted: 1987-03-27Accepted: 1987-06-26Date issued: 1988-09-15

Publication Status: Issued

Pages: 12

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Rev. Type: Peer

Identifiers: DOI: 10.1016/0008-6215(88)80074-0

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Title: Carbohydrate Research

Abbreviation : Carbohydr. Res.

Source Genre: Journal

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Publ. Info: Amsterdam : Elsevier

Pages: - Volume / Issue: 180 (2) Sequence Number: - Start / End Page: 163 - 174 Identifier: ISSN: 0008-6215
CoNE: https://pure.mpg.de/cone/journals/resource/954925388219