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  Aligned deuterochloroform in cross-linked polystyrene as a new sample for adjusting the magic angle in HR-MAS

Leutzsch, M., Findeisen, M., & Berger, S. (2012). Aligned deuterochloroform in cross-linked polystyrene as a new sample for adjusting the magic angle in HR-MAS. Magnetic Resonance in Chemistry, 50(1), 5-6. doi:10.1002/mrc.3789.

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Item Permalink: https://hdl.handle.net/21.11116/0000-000A-7127-B Version Permalink: https://hdl.handle.net/21.11116/0000-000A-7128-A
Genre: Journal Article

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 Creators:
Leutzsch, Markus1, Author           
Findeisen, Matthias1, Author
Berger, Stefan1, Author
Affiliations:
1Institut für Analytische Chemie, Universität Leipzig, Leipzig, Germany, ou_persistent22              

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Free keywords: magic angle; HR-MAS; polystyrene stick; alignment
 Abstract: A new and easily usable sample for adjusting the magic angle in a high resolution magic angle spinning (HR-MAS) probe head is a swollen polymer stick in CDCl3. The deuterium resonance shows a quadrupolar splitting if the rotor assembly is not at the magic angle, but a sharp singlet if the magic angle is correctly adjusted.

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Language(s): eng - English
 Dates: 2011-09-082012-01-232012-01-01
 Publication Status: Issued
 Pages: 2
 Publishing info: -
 Table of Contents: -
 Rev. Type: Peer
 Identifiers: DOI: 10.1002/mrc.3789
 Degree: -

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Title: Magnetic Resonance in Chemistry
  Abbreviation : Magn. Reson. Chem.
Source Genre: Journal
 Creator(s):
Affiliations:
Publ. Info: Hoboken, N.Y., USA : John Wiley & Sons
Pages: - Volume / Issue: 50 (1) Sequence Number: - Start / End Page: 5 - 6 Identifier: ISSN: 0749-1581
CoNE: https://pure.mpg.de/cone/journals/resource/954928503544