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  Complex transitions between dihydrate and anhydrate forms of ectoine - unexpected behavior of a highly hygroscopic compatible solute in the solid state

Hutzler, W. M., Mossou, E., Vollrath, R., Kohagen, M., El Ghrissi, I., Grininger, M., et al. (2020). Complex transitions between dihydrate and anhydrate forms of ectoine - unexpected behavior of a highly hygroscopic compatible solute in the solid state. CrystEngComm, 22(2), 169-172. doi:10.1039/c9ce01599j.

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Genre: Journal Article

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 Creators:
Hutzler, W. M., Author
Mossou, E., Author
Vollrath, R.1, Author              
Kohagen, M., Author
El Ghrissi, I., Author
Grininger, Martin, Author
Zaccai, G., Author
Smiatek, J., Author
Oesterhelt, D.1, Author              
Affiliations:
1Oesterhelt, Dieter / Membrane Biochemistry, Max Planck Institute of Biochemistry, Max Planck Society, ou_1565164              

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Free keywords: aqueous-solution protein binding Chemistry Crystallography
 Abstract: The crystalline dihydrate of the compatible solute ectoine undergoes a loss of water at ambient conditions and transforms into a highly hygroscopic anhydrate form. This unexpected transition is studied combining single-crystal and powder X-ray, single crystal neutron diffraction measurements and quantum mechanical calculations. Overall, our study provides a rationale for the important uptake and loss of water by ectoine in the solid state.

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Language(s): eng - English
 Dates: 2020
 Publication Status: Published in print
 Pages: -
 Publishing info: -
 Table of Contents: -
 Rev. Type: -
 Identifiers: Other: WOS:000507600600002
DOI: 10.1039/c9ce01599j
 Degree: -

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Title: CrystEngComm
  Other : CrystEngComm
Source Genre: Journal
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Publ. Info: London : Royal Society of Chemistry
Pages: - Volume / Issue: 22 (2) Sequence Number: - Start / End Page: 169 - 172 Identifier: ISSN: 1466-8033
CoNE: https://pure.mpg.de/cone/journals/resource/954928434986