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  Synthesis, Single-crystal Structure and Raman Spectrum of Cu[N(CN)2]2•2NH3

Reckeweg, O., Schulz, A., & DiSalvo, F. J. (2013). Synthesis, Single-crystal Structure and Raman Spectrum of Cu[N(CN)2]2•2NH3. Zeitschrift für Naturforschung B, 68(3), 296-300.

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Item Permalink: https://hdl.handle.net/21.11116/0000-000E-C575-0 Version Permalink: https://hdl.handle.net/21.11116/0000-000E-C576-F
Genre: Journal Article

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 Creators:
Reckeweg, O.1, Author           
Schulz, A.2, Author           
DiSalvo, F. J., Author
Affiliations:
1Former Departments, Max Planck Institute for Solid State Research, Max Planck Society, ou_3370502              
2Miscellaneous, Max Planck Institute for Solid State Research, Max Planck Society, ou_3370507              

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 Abstract: Transparent blue crystals of Cu[N(CN)(2)](2) center dot 2 NH3 were obtained by blending solutions of Na[N(CN)(2)] and Cu(NO3)(2) center dot 2.5 H2O in aqueous ammonia and subsequent evaporation of the solvent under ambient conditions. Cu[N(CN)(2)](2) center dot 2 NH3 crystallizes in space group P (1) over bar (no. 2, Z = 2) with the cell parameters a = 746.1(4), b = 747.8(4) and c = 894.4(5) pm, and the angles alpha = 68.94(2), beta = 75.52(1) and gamma = 68.22(4)degrees. The presence of the dicyanamide anion and the ammonia molecules was verified by Raman spectroscopy.

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Language(s): eng - English
 Dates: 2013
 Publication Status: Issued
 Pages: -
 Publishing info: -
 Table of Contents: -
 Rev. Type: Internal
 Identifiers: eDoc: 672223
ISI: 000318836000015
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Title: Zeitschrift für Naturforschung B
Source Genre: Journal
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Pages: - Volume / Issue: 68 (3) Sequence Number: - Start / End Page: 296 - 300 Identifier: ISSN: 0932-0776