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  Fe3Mo3N: Crystal Structure, High-Temperature Behavior, and Catalytic Activity for Ammonia Decomposition

Hund, S., Gómez-Cápiro, O., Dembélé, K., Berendts, S., Lunkenbein, T., Ruland, H., et al. (2023). Fe3Mo3N: Crystal Structure, High-Temperature Behavior, and Catalytic Activity for Ammonia Decomposition. Zeitschrift für anorganische und allgemeine Chemie, 649(20): e202300152. doi:10.1002/zaac.202300152.

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Item Permalink: https://hdl.handle.net/21.11116/0000-000E-51E1-8 Version Permalink: https://hdl.handle.net/21.11116/0000-000E-51E4-5
Genre: Journal Article

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Zeitschrift anorg allge chemie - 2023 - Hund - Fe3Mo3N Crystal Structure High‐Temperature Behavior and Catalytic.pdf (Publisher version), 2MB
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Zeitschrift anorg allge chemie - 2023 - Hund - Fe3Mo3N Crystal Structure High‐Temperature Behavior and Catalytic.pdf
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2023
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 Creators:
Hund, Sophie, Author
Gómez-Cápiro, Oscar, Author
Dembélé, Kassiogé1, Author                 
Berendts, Stefan, Author
Lunkenbein, Thomas1, Author                 
Ruland, Holger, Author
Heppke, Eva M., Author
Lerch, Martin, Author
Affiliations:
1Inorganic Chemistry, Fritz Haber Institute, Max Planck Society, ou_24023              

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 Abstract: Fe3Mo3N was synthesized successfully via ammonolysis out of an oxidic precursor prepared by a modified Pechini route. Rietveld refinement using X-ray powder data confirmed that the compound crystallizes in space group with a lattice parameter of a=11.0777 Å. Group theoretical methods were applied to elucidate the relation between the crystal structure of Fe3Mo3N and that of the copper type. The high temperature behavior of Fe3Mo3N in ammonia gas was investigated by in situ powder X-ray diffraction. In addition, the catalytic activity of our iron molybdenum nitride for ammonia decomposition was measured and compared to the activity of an industrial iron-based catalyst. Both catalysts show similar performances.

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Language(s): eng - English
 Dates: 2023-08-292023-07-052023-09-112023-10-16
 Publication Status: Issued
 Pages: 6
 Publishing info: -
 Table of Contents: -
 Rev. Type: Peer
 Identifiers: DOI: 10.1002/zaac.202300152
 Degree: -

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Title: Zeitschrift für anorganische und allgemeine Chemie
  Other : J. Inorg. Gen Chem.
  Other : Journal of Inorganic and General Chemistry
  Abbreviation : Z. Anorg. Allg. Chem.
Source Genre: Journal
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Publ. Info: Leipzig, Weinheim : Verlag Johann Ambrosius Barth / Wiley-VCH
Pages: 6 Volume / Issue: 649 (20) Sequence Number: e202300152 Start / End Page: - Identifier: Other: 1521-3749
ISSN: 0044-2313
CoNE: https://pure.mpg.de/cone/journals/resource/954925453895