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  Continuous flow oxidation of alkynes with KMnO4 for the synthesis of 1,2-diketone derivatives

Velichko, V., Cambié, D., & Secci, F. (2024). Continuous flow oxidation of alkynes with KMnO4 for the synthesis of 1,2-diketone derivatives. Reaction chemistry & engineering, 9(7), 1721-1725. doi:10.1039/D3RE00716B.

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Item Permalink: https://hdl.handle.net/21.11116/0000-000F-9751-B Version Permalink: https://hdl.handle.net/21.11116/0000-0010-3AD3-F
Genre: Journal Article

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 Creators:
Velichko, Viktoria1, Author
Cambié, Dario1, Author                 
Secci, Francesco, Author
Affiliations:
1Dario Cambié, Biomolekulare Systeme, Max Planck Institute of Colloids and Interfaces, Max Planck Society, ou_3256668              

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 Abstract: A continuous-flow process for the conversion of functionalized alkynes to 1,2-diketones and α-keto-carboxylic acids, using KMnO4 as the oxidizing agent has been developed. The simultaneous use of pulsed sonication combined with an in-line liquid–liquid separation process, avoids clogging of the microfluidic reactor by MnO2 slurries, ensuring reproducibility and high yields.

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Language(s): eng - English
 Dates: 2024-03-062024
 Publication Status: Issued
 Pages: -
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 Table of Contents: -
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 Identifiers: DOI: 10.1039/D3RE00716B
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Title: Reaction chemistry & engineering
  Abbreviation : React. Chem. Eng.
Source Genre: Journal
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Publ. Info: Cambridge : Royal Society of Chemistry
Pages: - Volume / Issue: 9 (7) Sequence Number: - Start / End Page: 1721 - 1725 Identifier: ISSN: 2058-9883