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  Efficient and flexible synthesis of chiral gamma- and delta-lactones

Habel, A., & Boland, W. (2008). Efficient and flexible synthesis of chiral gamma- and delta-lactones. Organic & Biomolecular Chemistry, 6(9), 1601-1604. doi:10.1039/b801514g.

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Item Permalink: https://hdl.handle.net/11858/00-001M-0000-0012-A03F-8 Version Permalink: https://hdl.handle.net/21.11116/0000-0009-3570-D
Genre: Journal Article

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BOL452s1.pdf (Supplementary material), 2MB
 
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 Creators:
Habel, A.1, Author           
Boland, W.1, Author           
Affiliations:
1Department of Bioorganic Chemistry, MPI for Chemical Ecology, Max Planck Society, ou_24028              

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Free keywords: Hydrolytic kinetic resolution Baeyer-villiger oxidations Terminal epoxides Sesquiterpene lactones Organic-solvents Building-blocks Pheromones Cleavage 3,4-dihydroisocoumarins Butyrolactones Chemistry & Analysis in Current Contents(R)/Life Sciences Organic Chemistry/Polymer Science in Current Contents(R)/Physical, Chemical & Earth Sciences
 Abstract: An efficient and highly flexible synthesis for chiral gamma- and delta-lactones with high enantiomeric purity is described (> 99% ee and 57-87% overall yield). The protocol involves alkylation of chiral 1,2-oxiranes with terminally unsaturated Grignard

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 Dates: 2008
 Publication Status: Issued
 Pages: -
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 Rev. Type: -
 Identifiers: Other: BOL452
DOI: 10.1039/b801514g
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Title: Organic & Biomolecular Chemistry
  Other : Organic and Biomolecular Chemistry
  Abbreviation : Org. Biomol. Chem.
Source Genre: Journal
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Publ. Info: Cambridge : Royal Society of Chemistry
Pages: - Volume / Issue: 6 (9) Sequence Number: - Start / End Page: 1601 - 1604 Identifier: ISSN: 1477-0520
CoNE: https://pure.mpg.de/cone/journals/resource/954925269322