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  Microwave-Assisted Self-Propagating Combustion Synthesis for Uniform Deposition of Metal Nanoparticles on Ceramic Monoliths

Zavyalova, U., Girgsdies, F., Korup, O., Horn, R., & Schlögl, R. (2009). Microwave-Assisted Self-Propagating Combustion Synthesis for Uniform Deposition of Metal Nanoparticles on Ceramic Monoliths. Journal of Physical Chemistry C, 113(40), 17493-17501. doi:10.1021/jp905692g.

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 Creators:
Zavyalova, Ulyana1, Author           
Girgsdies, Frank1, Author           
Korup, Oliver1, Author           
Horn, Raimund1, Author           
Schlögl, Robert1, Author           
Affiliations:
1Inorganic Chemistry, Fritz Haber Institute, Max Planck Society, ou_24023              

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Free keywords: nanoparticles; microwave radiation; High temperature catalysis research
 Abstract: A new microwave-assisted gel-combustion synthesis in self-propagating mode was developed for the deposition of adhesive metal nanoparticles on ceramic substrates. Pt particles with diameters less than 10 nm uniformly distributed on corundum foams were prepared by the fast and reliable combustion method with no additional calcination or reduction steps. The results are rationalized in terms of the exothermic combustion of the glycerol-chelated metal precursor and subsequent in situ reduction assisted by the formed amorphous carbon absorbing microwave radiation.

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Language(s): eng - English
 Dates: 2009-06
 Publication Status: Published in print
 Pages: -
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 Table of Contents: -
 Rev. Type: Peer
 Identifiers: DOI: 10.1021/jp905692g
 Degree: -

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Title: Journal of Physical Chemistry C
  Alternative Title : J. Phys. Chem. C
Source Genre: Journal
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Pages: - Volume / Issue: 113 (40) Sequence Number: - Start / End Page: 17493 - 17501 Identifier: -