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  Synthesis and investigations of rutile phase nanoparticles of TiO2

Borse, P. H., Kankate, L. S., Dassenoy, F., Vogel, W., Urban, J., & Kulkarni, S. K. (2002). Synthesis and investigations of rutile phase nanoparticles of TiO2. Journal of Materials Science: Materials in Electronics, 13(9), 553-559. doi:10.1023/A:1019677730981.

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 Creators:
Borse, P. H., Author
Kankate, Laxman S., Author
Dassenoy, Fabrice1, Author           
Vogel, Walter1, Author           
Urban, Joachim2, Author           
Kulkarni, Sulabha K., Author
Affiliations:
1Molecular Physics, Fritz Haber Institute, Max Planck Society, ou_634545              
2Inorganic Chemistry, Fritz Haber Institute, Max Planck Society, ou_24023              

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Free keywords: TITANIUM-DIOXIDE; SOLAR-CELLS; PHOTOCATALYTIC OXIDATION; SIZE QUANTIZATION; ANATASE TIO2; SEMICONDUCTOR; FILMS; PRECIPITATION; NANOCRYSTALS; POLYMER
 Abstract: TiO2 nanoparticles have been synthesized at room temperature using a simple chemical precipitation route. Particles were further coated with polymer. Detailed structural analysis of the particles has been carried out. Wide-angle X-ray scattering (WAXS) and transmission electron microscopy (TEM) confirm that "as-synthesized" particles as well as annealed particles are nanoparticles having pure rutile phase. Thermal annealing at 1000 degreesC of 4.2 nm particles led to an increased size similar to20 nm in the same phase. The purity and composition of the particles were determined using energy dispersive analysis of X-rays (EDAX) and X-ray photoelectron spectroscopy (XPS), respectively.

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Language(s): eng - English
 Dates: 2002-09
 Publication Status: Issued
 Pages: -
 Publishing info: -
 Table of Contents: -
 Rev. Type: Peer
 Identifiers: eDoc: 8335
DOI: 10.1023/A:1019677730981
 Degree: -

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Title: Journal of Materials Science: Materials in Electronics
  Alternative Title : J. Mater. Sci. - Mater. El.
Source Genre: Journal
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Pages: - Volume / Issue: 13 (9) Sequence Number: - Start / End Page: 553 - 559 Identifier: -