Direct synthesis of pure complex aluminium hydrides by cryomilling

Pommerin, André; Weidenthaler, Claudia; Schüth, Ferdi; Felderhoff, Michael

doi:10.1016/j.scriptamat.2009.12.041

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Direct synthesis of pure complex aluminium hydrides by cryomilling

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Pommerin, André
Research Department Schüth, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Weidenthaler, Claudia
Research Department Schüth, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Schüth, Ferdi
Research Department Schüth, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Felderhoff, Michael
Research Department Schüth, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Citation

Pommerin, A., Weidenthaler, C., Schüth, F., & Felderhoff, M. (2010). Direct synthesis of pure complex aluminium hydrides by cryomilling. Scripta Materialia, 62(8), 576-578. doi:10.1016/j.scriptamat.2009.12.041.

Cite as: https://hdl.handle.net/11858/00-001M-0000-000F-8DE7-9

Abstract

Simple mechanochemical procedures can be used for the solid-state preparation of stable complex aluminium hydrides as hydrogen storage materials. For the synthesis of unstable complex hydrides, cryomilling at temperatures at which product decomposition does not take place under milling conditions appears to be a viable method. To probe the potential of cryomilling for the synthesis of complex aluminium hydrides, the reactions of different alkaline hydrides with AlH₃ were tested under these conditions.