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Mechanochemical Synthesis of Ternary Potassium Transition Metal Chlorides

MPS-Authors
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Pawelke,  Roland H.
Research Department Schüth, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Felderhoff,  Michael
Research Department Schüth, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Weidenthaler,  Claudia
Research Department Schüth, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Bogdanović,  B.
Research Group Bogdanovi?, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Schüth,  Ferdi
Research Department Schüth, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Citation

Pawelke, R. H., Felderhoff, M., Weidenthaler, C., Bogdanović, B., & Schüth, F. (2009). Mechanochemical Synthesis of Ternary Potassium Transition Metal Chlorides. Zeitschrift für anorganische und allgemeine Chemie, 635(2), 265-270. doi:10.1002/zaac.200800416.


Cite as: http://hdl.handle.net/11858/00-001M-0000-000F-8F2F-8
Abstract
Ternary halide systems KMIICl3 (MII = Ti, Cr, Mn, Fe, Co, Ni, Cu, Zn) have been prepared by mechanochemical synthesis. Furthermore, TiCl2 was converted to Ti7Cl16 by mechanochemical treatment. For most samples, the X‐ray powder diffraction patterns could either be assigned to isotypic structures or were found in accordance with reference data. The monochloride systems of Ti, Co and Zn were extended to their double chloride stoichiometry K2MIICl4.