English
 
Help Privacy Policy Disclaimer
  Advanced SearchBrowse

Item

ITEM ACTIONSEXPORT
Add to Basket
  Local TagsRelease HistoryDetailsSummary

Released
Journal Article

Heterogeneous Catalysis under pressure - In-situ neutron diffraction under industrial conditions

MPS-Authors
/persons/resource/persons21695

Kandemir,  Timur
Inorganic Chemistry, Fritz Haber Institute, Max Planck Society;

/persons/resource/persons21557

Girgsdies,  Frank
Inorganic Chemistry, Fritz Haber Institute, Max Planck Society;

/persons/resource/persons21700

Kasatkin,  Igor
Inorganic Chemistry, Fritz Haber Institute, Max Planck Society;

/persons/resource/persons21779

Kunkes,  Edward L.
Inorganic Chemistry, Fritz Haber Institute, Max Planck Society;

/persons/resource/persons22071

Schlögl,  Robert
Inorganic Chemistry, Fritz Haber Institute, Max Planck Society;

/persons/resource/persons21347

Behrens,  Malte
Inorganic Chemistry, Fritz Haber Institute, Max Planck Society;

External Resource
No external resources are shared
Fulltext (restricted access)
There are currently no full texts shared for your IP range.
Fulltext (public)

1742-6596_340_1_012053.pdf
(Publisher version), 2MB

Supplementary Material (public)
There is no public supplementary material available
Citation

Kandemir, T., Girgsdies, F., Kasatkin, I., Kunkes, E. L., Liss, K.-D., Peterson, V. K., et al. (2012). Heterogeneous Catalysis under pressure - In-situ neutron diffraction under industrial conditions. Journal of Physics: Conference Series, 340(1): 012053. doi:10.1088/1742-6596/340/1/012053.


Cite as: https://hdl.handle.net/11858/00-001M-0000-0010-1F08-B
Abstract
The present work describes the application of a tubular reactor that allows in-situ neutron diffraction on working catalysts at high pressures. The designed reactor enables the application to a sample of industrially-relevant reaction conditions, i.e., in a temperature range up to 330° C and 60 bar pressure, coupled with online gas-analysis. Application of the cell is demonstrated by ammonia synthesis over a commercial catalyst with diffraction data obtained from the high-resolution powder diffractometer, Echidna, at the Australian Nuclear Science and Technology Organisation, ANSTO.