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Thermokinetic study of the reduction process of a CuO/ZnAl2O4 catalyst

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Tarasov,  Andrey
Inorganic Chemistry, Fritz Haber Institute, Max Planck Society;

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Kühl,  Stefanie
Inorganic Chemistry, Fritz Haber Institute, Max Planck Society;

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Schumann,  Julia
Inorganic Chemistry, Fritz Haber Institute, Max Planck Society;

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Behrens,  Malte
Inorganic Chemistry, Fritz Haber Institute, Max Planck Society;

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Citation

Tarasov, A., Kühl, S., Schumann, J., & Behrens, M. (2013). Thermokinetic study of the reduction process of a CuO/ZnAl2O4 catalyst. High Temperatures-High Pressures, 42(4), 377-386. Retrieved from http://www.oldcitypublishing.com/HTHP/HTHPcontents/HTHP42.4contents.html.


Cite as: https://hdl.handle.net/11858/00-001M-0000-0013-FAEB-8
Abstract
Formal kinetic analysis of reduction process of the Cu-based layered double hydroxide – LDH catalyst precursor for methanol synthesys was implemented. The process was studied by means of thermogravimetry (TG) and Differential scanning calorimetry (DSC) with respect to changes taking place in gas phase, which was analyzed by Massspectrometry (MS). The kinetic parameters of the non-isothermal reduction were determined and the rate limiting step was found.