Multinuclear (11B, 31P) MAS NMR spectroscopy of borophosphates

Grimmer, A.-R.; Müller, D.; Gözel, G.; Kniep, R.

doi:10.1007/s002160050197

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Multinuclear (¹¹B, ³¹P) MAS NMR spectroscopy of borophosphates

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Grimmer, A.-R., Müller, D., Gözel, G., & Kniep, R. (1997). Multinuclear (¹¹B, ³¹P) MAS NMR spectroscopy of borophosphates. Fresenius' Journal of Analytical Chemistry, 357(5), 485-488. doi:10.1007/s002160050197.

Cite as: https://hdl.handle.net/11858/00-001M-0000-0019-BDFE-7

Abstract

B-11 and P-31 MAS NMR spectroscopy of three borophosphates was used to monitor their phase composition via the isotropic chemical shifts. CaBPO5 and BPO4 represent nearly pure samples, SrBPO5 contains beta-Sr2P2O7 as well as BPO4 as impurities. The anisotropic chemical shift data provide additional information on the geometry and connectivity of the BO4 and PO4 building units.