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Synthese und Reactivität von (2,6-iPr2Ph-dad)Ni(C2F4)

MPS-Authors

Schröder,  Wolfgang
Max-Planck-Institut für Kohlenforschung, Max Planck Society;

Bonrath,  Werner
Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Pörschke,  Klaus-Richard
Research Group Pörschke, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Citation

Schröder, W., Bonrath, W., & Pörschke, K.-R. (1991). Synthese und Reactivität von (2,6-iPr2Ph-dad)Ni(C2F4). Journal of Organometallic Chemistry, 408(2), C25-C29. doi:10.1016/0022-328X(91)86393-5.


Cite as: http://hdl.handle.net/11858/00-001M-0000-0024-47CC-5
Abstract
Upon warming the reaction mixture of Ni(cdt), C2F4, and 2,6-iPr2Ph-dad in THF from - 78-degrees-C to room temperature the red-violet complex (2,6-iPr2Ph-dad)Ni(C2F4) (1) is obtained. 1 reacts with ethene already at - 78-degrees-C by coupling of the olefinic ligands with the nickel atom to form the blue nickelatetrafluoro-cyclopentane compound (2,6-iPr2Ph-dad)Ni(C2H4C2F4) (2).