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Speciation in Solution: Silicate Oligomers in Aqueous Solutions Detected by Mass Spectrometry

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Bussian,  P.
Research Department Schüth, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Schrader,  Wolfgang
Service Department Schrader (MS), Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Schüth,  F.
Research Department Schüth, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Citation

Bussian, P., Sobott, F., Brutschy, B., Schrader, W., & Schüth, F. (2000). Speciation in Solution: Silicate Oligomers in Aqueous Solutions Detected by Mass Spectrometry. Angewandte Chemie International Edition: a journal of the Gesellschaft Deutscher Chemiker, 39(21), 3901-3905. doi:10.1002/1521-3773(20001103)39:21<3901:AID-ANIE3901>3.0.CO;2-D.


Cite as: http://hdl.handle.net/11858/00-001M-0000-0024-3BF0-3
Abstract
Electrospray mass spectrometry has been used for the first time to analyze inorganic oligomeric species in aqueous solutions. Different double-four rings and double-three rings could be reliably analyzed in silicate solutions, as proven by independent29Si NMR spectroscopy. This technique might prove valuable in the analysis of nucleating solutions.