Formation of a Porous Zirconium Oxo Phosphate with a High Surface Area by a 
Surfactant-Assisted Synthesis

Ciesla, U.; Schacht, S.; Stucky, G.D.; Unger, K.K.; Schüth, F.

doi:10.1002/anie.199605411

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Formation of a Porous Zirconium Oxo Phosphate with a High Surface Area by a Surfactant-Assisted Synthesis

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Schüth, F.
Institut für Anorganische Chemie der Universität, Marie-Curie-Strasse 11, D-60439 Frankfurt (Germany) ;
Research Department Schüth, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Citation

Ciesla, U., Schacht, S., Stucky, G., Unger, K., & Schüth, F. (1996). Formation of a Porous Zirconium Oxo Phosphate with a High Surface Area by a Surfactant-Assisted Synthesis. Angewandte Chemie International Edition, 35(5), 541-543. doi:10.1002/anie.199605411.

Cite as: https://hdl.handle.net/11858/00-001M-0000-0024-36F2-5

Abstract

Analogous to the synthesis of MCM-41, a mesostructured product (shown schematically on the right) can be obtained from aqueous solutions of zirconium sulfate by addition of alkyltrimethylammonium salts. After a treatment with phosphoric acid, this material can be calcined without structural collapse. The resulting zirconium oxo phosphate shows BET surface areas of up to 400 m² g⁻¹.