The theoretical and practical limits of resolution in multiple-pulse 
high-resolution NMR of solids

Prigl, R.; Haeberlen, Ulrich

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The theoretical and practical limits of resolution in multiple-pulse high-resolution NMR of solids

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Haeberlen, Ulrich
Research Group Prof. Dr. Haeberlen, Max Planck Institute for Medical Research, Max Planck Society;

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http://www.sciencedirect.com/science?_ob=MiamiImageURL&_cid=276000&_user=41901&_pii=S1057273296800179&_check=y&_origin=article&_zone=toolbar&_coverDate=31-Dec-1996&view=c&originContentFamily=serial&wchp=dGLzVlk-zSkWb&md5=34f5c04570978d46511ef13b8e17887f&pid=1-s2.0-S1057273296800179-main.pdf
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http://dx.doi.org/10.1016/S1057-2732(96)80017-9
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Prigl, R., & Haeberlen, U. (1996). The theoretical and practical limits of resolution in multiple-pulse high-resolution NMR of solids. Advances in Magnetic and Optical Resonance, 19, 1-58.

Cite as: https://hdl.handle.net/11858/00-001M-0000-0024-37F0-1

Abstract

This chapter discusses the theoretical and practical limits of resolution in multiple-pulse (m.p.) high-resolution nuclear magnetic resonance (NMR) of solids. m.p. M.P sequences for high-resolution (NMR) in solids were introduced in 1968 by the MIT NMR group. Experimentalists working on the advance of high-resolution NMR in solids have been frustrated over many years by the apparent existence of a "magic wall" that prevented them from improving the resolution in their m.p. spectra beyond a certain limit. The purpose of this report is to explore, on the one hand, the theoretical and, on the other, the practical limitations of high-resolution solid state proton and fluorine NMR.