Crystal structure redetermination of the D,L-glyceraldehyde dimer: A comparison 
of synchrotron and conventional X-ray diffraction data

Lehmann, Christian W.; Luger, Peter

doi:10.1524/zkri.1991.195.1-2.49

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Crystal structure redetermination of the D,L-glyceraldehyde dimer: A comparison of synchrotron and conventional X-ray diffraction data

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Lehmann, C. W., & Luger, P. (1991). Crystal structure redetermination of the D,L-glyceraldehyde dimer: A comparison of synchrotron and conventional X-ray diffraction data. Zeitschrift für Kristallographie-Crystalline Materials, 195(1-2), 49-63. doi:10.1524/zkri.1991.195.1-2.49.

Cite as: https://hdl.handle.net/11858/00-001M-0000-0024-C263-C

Abstract

The structure of D,L-glyceraldehyde has been redetermined by means of synchrotron and conventional X-radiation. At 295 K lattice parameters in monoclinic space group P2₁/n are: a=6.403(2)Å, b= 6.961(2)Å, c=8.830(3)Å, beta=105.00(2)°, V=380.12Å³, Z=2. Three independent data sets of crystals with
crystal volumes of 0.00009 and 0.02mm³ are compared. As a main advantage of the synchrotron experiment it was found that its results obtained with the small crystal are of similar precision compared to those based on the larger crystal measured with a conventional tube.