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One-step synthesis of a cyclic 2,17-dioxo[3,3](4,4′) biphenylophane and first preparation of a microporous polymer network from a macrocyclic precursor by cyclotrimerization

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Lehmann,  Christian W.
Service Department Lehmann (EMR), Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Goddard,  Richard
Service Department Lehmann (EMR), Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Citation

Samanta, S. K., Preis, E., Lehmann, C. W., Goddard, R., Bag, S., Maiti, P. K., et al. (2015). One-step synthesis of a cyclic 2,17-dioxo[3,3](4,4′) biphenylophane and first preparation of a microporous polymer network from a macrocyclic precursor by cyclotrimerization. Chemical Communications, 51(43), 9046-9049. doi:10.1039/C5CC01654A.


Cite as: http://hdl.handle.net/11858/00-001M-0000-0027-B2B0-5
Abstract
One-step synthesis of a cyclic 2,17-dioxo[3,3](4,40)biphenylophane (MC) was achieved in high yield; its structure was verified by single crystal X-ray analysis. As a first example, a microporous polymer network was formed from macrocycle MC via acid-catalysed cyclotrimerization yielding a BET surface area of ca. 570 m2 g-1.