Correlation of deuterium quadrupolar couplings and carbon-13 chemical shifts in 
ordered media by multiple-quantum NMR

Sandström, Dick; Zimmermann, Herbert

doi:10.1021/jp9938765

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Correlation of deuterium quadrupolar couplings and carbon-13 chemical shifts in ordered media by multiple-quantum NMR

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Zimmermann, Herbert
Emeritus Group Biophysics, Max Planck Institute for Medical Research, Max Planck Society;

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Sandström, D., & Zimmermann, H. (2000). Correlation of deuterium quadrupolar couplings and carbon-13 chemical shifts in ordered media by multiple-quantum NMR. The Journal of Physical Chemistry B, 104(7), 1490-1493. doi:10.1021/jp9938765.

Cite as: https://hdl.handle.net/11858/00-001M-0000-0028-1ADA-6

Abstract

We report a simple and robust NMR approach capable of correlating deuterium quadrupolar splittings with carbon−13 chemical shifts in oriented materials. The technique, which is based on heteronuclear multiple−quantum spectroscopy, results in two−dimensional maps that are very useful for the assignment of deuterium NMR spectra. The experiment has been employed to measure and assign all quadrupolar couplings produced by a perdeuterated liquid crystal