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Access to side-chain carbon information in deuterated solids under fast MAS through non-rotor-synchronized mixing.

MPG-Autoren
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Kulminskaya,  N.
Department of NMR-Based Structural Biology, MPI for biophysical chemistry, Max Planck Society;

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Vasa,  S. K.
Research Group of Solid-State NMR-2, MPI for Biophysical Chemistry, Max Planck Society;

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Giller,  K.
Department of NMR-Based Structural Biology, MPI for biophysical chemistry, Max Planck Society;

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Becker,  S.
Department of NMR-Based Structural Biology, MPI for biophysical chemistry, Max Planck Society;

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Linser,  R.
Research Group of Solid-State NMR-2, MPI for Biophysical Chemistry, Max Planck Society;

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Zitation

Kulminskaya, N., Vasa, S. K., Giller, K., Becker, S., Kwan, A., Sunde, M., et al. (2016). Access to side-chain carbon information in deuterated solids under fast MAS through non-rotor-synchronized mixing. Chemical Communications, 52(2), 268-271. doi:10.1039/C5CC07345F.


Zitierlink: http://hdl.handle.net/11858/00-001M-0000-0028-EA2C-3
Zusammenfassung
We demonstrate the accessibility of aliphatic 13C side chain chemical shift sets for solid-state NMR despite perdeuteration and fast MAS using isotropic, non-rotor-synchronized 13C-13C mixing. Combined with amide proton detection, we unambiguously and sensitively detect whole side chain to backbone correlations for two proteins using around 1 mg of sample.