AlkylFluor: Deoxyfluorination of Alcohols

Goldberg, Nathaniel W.; Shen, Xiao; Li, Jiantung; Ritter, Tobias

doi:10.1021/acs.orglett.6b03086

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AlkylFluor: Deoxyfluorination of Alcohols

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Li, Jiantung
Department of Chemistry and Chemical Biology, Harvard University;
Research Department Ritter, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Ritter, Tobias
Department of Chemistry and Chemical Biology, Harvard University;
Research Department Ritter, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Citation

Goldberg, N. W., Shen, X., Li, J., & Ritter, T. (2016). AlkylFluor: Deoxyfluorination of Alcohols. Organic Letters, 18(23), 6102-6104. doi:10.1021/acs.orglett.6b03086.

Cite as: https://hdl.handle.net/11858/00-001M-0000-002C-463F-E

Abstract

A practical, high-yielding method for the deoxy-fluorination of alcohols is presented using AlkylFluor, a novel salt analogue of PhenoFluor. AlkylFluor is readily prepared on multigram scale and is stable to long-term storage in air and exposure to water. The practicality and applicability of this method is demonstrated with a variety of primary and secondary alcohol substrates.