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Journal Article

Controlled mineralization and assembly of hydrolysis-based nanoparticles in organic solvents combining polymer micelles and microwave techniques

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Spatz,  Joachim
Cellular Biophysics, Max Planck Institute for Medical Research, Max Planck Society;
Biophysical Chemistry, Institute of Physical Chemistry, University of Heidelberg, 69120 Heidelberg, Germany;

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http://onlinelibrary.wiley.com/doi/10.1002/(SICI)1521-4095(199804)10:6%3C473::AID-ADMA473%3E3.0.CO;2-Q/epdf
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Citation

Spatz, J., Mößmer, S., Möller, M., Kocher, M., Neher, D., & Wegner, G. (1998). Controlled mineralization and assembly of hydrolysis-based nanoparticles in organic solvents combining polymer micelles and microwave techniques. Advanced Materials Interfaces, 10, 473-475. doi:10.1002/(SICI)1521-4095(199804)10:6<473:AID-ADMA473>3.0.CO;2-Q.


Cite as: https://hdl.handle.net/11858/00-001M-0000-002A-66C1-6
Abstract
Controlled formation of nanoparticles in inverse diblock copolymer micelles by hydrolysis of titanium alkoxide precursors is described. Coagulation of the resulting TiO2-loaded micelles occurs on casting if the sample is prepared by conventional heating, allowing strings of TiO2 particles to form (see Figure). It is demonstrated that this can be prevented by microwave heating.