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Fourier transform pure nuclear quadrupole resonance by pulsed field cycling

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Zimmermann,  Herbert
Department of Molecular Physics, Max Planck Institute for Medical Research, Max Planck Society;
Department of Biomolecular Mechanisms, Max Planck Institute for Medical Research, Max Planck Society;
Zimmermann Group, Max Planck Institute for Medical Research, Max Planck Society;
Emeritus Group Biophysics, Max Planck Institute for Medical Research, Max Planck Society;

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Citation

Bielecki, A., Murdoch, J. B., Weitekamp, D. P., Zax, D. B., Zilm, K. W., Zimmermann, H., et al. (1984). Fourier transform pure nuclear quadrupole resonance by pulsed field cycling. The Journal of Chemical Physics, 80(5), 2232-2234. doi:10.1063/1.446915.


Cite as: http://hdl.handle.net/21.11116/0000-0000-D4E1-2
Abstract
We report the observation of Fourier transform pure NQR by pulsed field cycling. For deuterium, well resolved spectra are obtained with high sensitivity showing the low frequency ν0 lines and allowing assignments of quadrupole couplings and asymmetry parameters to inequivalent deuterons. The technique is ideally applicable to nuclei with low quadrupolar frequencies (e.g., 2D, 7Li, 11B, 27Al, 23Na, 14N) and makes possible high resolution structure determination in polycrystalline or disordered materials.