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Synthesis, structural and magnetic characterization of soft magnetic nanocrystalline ternary FeNiCo particles

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Toparli,  Cigdem
Interface Spectroscopy, Interface Chemistry and Surface Engineering, Max-Planck-Institut für Eisenforschung GmbH, Max Planck Society;
Department of Metallurgical & Materials Eng., Istanbul Technical University, Istanbul, Turkey;

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Citation

Toparli, C., Ebin, B., & Gürmen, S. (2017). Synthesis, structural and magnetic characterization of soft magnetic nanocrystalline ternary FeNiCo particles. Journal of Magnetism and Magnetic Materials, 423, 133-139. doi:10.1016/j.jmmm.2016.09.005.


Cite as: http://hdl.handle.net/21.11116/0000-0001-70DA-B
Abstract
The present study focuses on the synthesis, microstructural and magnetic properties of ternary FeNiCo nanoparticles. Nanocrystalline ternary FeNiCo particles were synthesized via hydrogen reduction assisted ultrasonic spray pyrolysis method in single step. The effect of precursor concentration on the morphology and the size of particles was investigated. The syntheses were performed at 800 degrees C. Structure, morphology and magnetic properties of the as-prepared products were characterized through X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and vibrating sample magnetometer (VSM) studies. Scherer calculation revealed that crystallite size of the ternary particles ranged between 36 and 60 nm. SEM and TEM investigations showed that the particle size was strongly influenced by the precursor concentration and Fe, Ni, Co elemental composition of individual particles was homogeneous. Finally, the soft magnetic properties of the particles were observed to be a function of their size.