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Nitroxide radicals. Part 19. Nuclear magnetic resonance study of [2,2]paracyclophan-4-yl t-butyl nitroxide

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Neugebauer,  Franz A.
Department of Organic Chemistry, Max Planck Institute for Medical Research, Max Planck Society;

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Fischer,  Hans
Department of Organic Chemistry, Max Planck Institute for Medical Research, Max Planck Society;

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Citation

Forrester, A. R., Neugebauer, F. A., & Fischer, H. (1978). Nitroxide radicals. Part 19. Nuclear magnetic resonance study of [2,2]paracyclophan-4-yl t-butyl nitroxide. Journal of the chemical Society, Perkin Transactions 2, 1978, 1014-1016. doi:10.1039/P29780001014.


Cite as: http://hdl.handle.net/21.11116/0000-0003-02DB-4
Abstract
N.m.r. measurements on specifically deuteriated [2,2]paracyclophan-4-yl t-butyl nitroxides and 4,12-[2,2]paracyclophanylene NN′-di-t-butyl bisnitroxide give clear assignments of the proton hyperfine coupling constants. There is no substantial interaction of the unpaired electron with transannular protons.