[1.n]Paracyclophane durch Vakuum‐Gasphasen‐Pyrolyse von Disulfonen

Ruland, Alfred; Staab, Heinz A.

doi:10.1002/cber.19781110828

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[1.n]Paracyclophane durch Vakuum‐Gasphasen‐Pyrolyse von Disulfonen

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Ruland, Alfred
Max Planck Institute for Medical Research, Max Planck Society;

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Staab, Heinz A.
Department of Organic Chemistry, Max Planck Institute for Medical Research, Max Planck Society;

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Citation

Ruland, A., & Staab, H. A. (1978). [1.n]Paracyclophane durch Vakuum‐Gasphasen‐Pyrolyse von Disulfonen. Chemische Berichte, 111(8), 2997-3000. doi:10.1002/cber.19781110828.

Cite as: https://hdl.handle.net/21.11116/0000-0003-031C-B

Abstract

By vacuum vapour phase pyrolysis of the cyclic disulfones 7–9 at 580 C 0.01 Torr the sterically strained [1.n]paracyclophanes 1–3 were obtained in excellent yields. The lowest members of this series 1 (n=5) and 2 (n=6) were not accessible by other methods so far.