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A versatile liquid-jet setup for the European XFEL1

MPG-Autoren
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Doak,  Bruce
Department of Biomolecular Mechanisms, Max Planck Institute for Medical Research, Max Planck Society;
Coherent diffractive imaging, Max Planck Institute for Medical Research, Max Planck Society;

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Shoeman,  Robert L.
Department of Biomolecular Mechanisms, Max Planck Institute for Medical Research, Max Planck Society;
Coherent diffractive imaging, Max Planck Institute for Medical Research, Max Planck Society;
Analytical Protein Biochemistry, Max Planck Institute for Medical Research, Max Planck Society;

Externe Ressourcen

https://onlinelibrary.wiley.com/doi/pdf/10.1107/S1600577519000894
(beliebiger Volltext)

https://doi.org/10.1107/S1600577519000894
(beliebiger Volltext)

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Zitation

Schulz, J., Bielecki, J., Doak, B., Dörner, K., Graceffa, R., Shoeman, R. L., et al. (2019). A versatile liquid-jet setup for the European XFEL1. Journal of Synchrotron Radiation, 26(2), 339-345. doi:10.1107/S1600577519000894.


Zitierlink: https://hdl.handle.net/21.11116/0000-0003-7829-9
Zusammenfassung
The SPB/SFX instrument of the European XFEL provides unique possibilities for high-throughput serial femtosecond crystallography. This publication presents the liquid-jet sample delivery setup of this instrument. The setup is compatible with state-of-the-art gas dynamic virtual nozzle systems as well as high-viscosity extruders and provides space and flexibility for other liquid injection devices and future upgrades. The liquid jets are confined in a differentially pumped catcher assembly and can be replaced within a couple of minutes through a load-lock. A two-microscope imaging system allows visual control of the jets from two perspectives.