Synthesis of photolabile protecting group (PPG) protected uronic acid building 
blocks : applications in carbohydrate synthesis with the assistance of a 
continuous flow photoreactor

Tiwari, Varsha; Singh, Adesh Kumar; Chaudhary, Priyanka; Seeberger, Peter H.; Kandasamy, Jeyakumar

doi:10.1039/C9QO01010F

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Synthesis of photolabile protecting group (PPG) protected uronic acid building blocks : applications in carbohydrate synthesis with the assistance of a continuous flow photoreactor

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Seeberger, Peter H.
Peter H. Seeberger - Vaccine Development, Biomolekulare Systeme, Max Planck Institute of Colloids and Interfaces, Max Planck Society;

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Citation

Tiwari, V., Singh, A. K., Chaudhary, P., Seeberger, P. H., & Kandasamy, J. (2019). Synthesis of photolabile protecting group (PPG) protected uronic acid building blocks: applications in carbohydrate synthesis with the assistance of a continuous flow photoreactor. Organic Chemistry Frontiers, 6, 3859-3863. doi:10.1039/C9QO01010F.

Cite as: https://hdl.handle.net/21.11116/0000-0005-4E67-1

Abstract

Photolabile protecting group (PPG) protected uronic acid building blocks were prepared and used for carbohydrate synthesis. Deprotection of the photolabile protecting group was achieved very efficiently by employing a continuous flow photoreactor under neutral conditions. Many conventional protecting groups were found to be stable during the photo-cleavage of the 2-nitrobenzyl group at 355 nm in methanol.