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Journal Article

An Approach to Chemical Reaction Engineering and Process Intensification for the Lean Aqueous Hydroformylation Using a Jet Loop Reactor

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Esteban,  Jesus
Research Department Leitner, Max Planck Institute for Chemical Energy Conversion, Max Planck Society;

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Vorholt,  Andreas J.
Research Department Leitner, Max Planck Institute for Chemical Energy Conversion, Max Planck Society;

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Citation

Esteban, J., Warmeling, H., & Vorholt, A. J. (2019). An Approach to Chemical Reaction Engineering and Process Intensification for the Lean Aqueous Hydroformylation Using a Jet Loop Reactor. Chemie-Ingenieur-Technik, 91(91), 560-566. doi:10.1002/cite.201800137.


Cite as: https://hdl.handle.net/21.11116/0000-0005-D45D-4
Abstract
The biphasic hydroformylation of 1-octene using a lean aqueous phase as solvent phase for catalyst recycling is discussed here. The gas-liquid-liquid reaction was homogeneously catalyzed by industrial standard catalytic system with [Rh(cod)Cl](2) as precursor and TPPTS as ligand. This work summarizes investigations addressing different aspects of the reaction, where a procedural approach was followed to gain understanding of its nature, kinetics and interphase reactivity. Finally, the application of the jet loop reactor is analyzed as a means to intensify the reaction.