Synthese von α‐Oxo‐ und α‐Hydrazono[1. n]paracyclophanen

Staab, Heinz A.; Alt, Reinhold

doi:10.1002/cber.19841170236

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Synthese von α‐Oxo‐ und α‐Hydrazono[1. n]paracyclophanen

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Staab, Heinz A.
Department of Organic Chemistry, Max Planck Institute for Medical Research, Max Planck Society;

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Alt, Reinhold
Max Planck Institute for Medical Research, Max Planck Society;

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Citation

Staab, H. A., & Alt, R. (1984). Synthese von α‐Oxo‐ und α‐Hydrazono[1. n]paracyclophanen. Chemische Berichte, 117(2), 850-855. doi:10.1002/cber.19841170236.

Cite as: https://hdl.handle.net/21.11116/0000-0005-A495-9

Abstract

α‐Oxo[1. n]paracyclophanes 1a – e (n = 12 – 8) were synthesized via the corresponding dithia‐[1. n]paracyclophanes 5a – e and the disulfones 6a – e derived therefrom. Spectroscopic properties (IR 13C NMR) and chemical reactivity of 1a – e are discussed in relation to the specific sterical structure of these diarylketones. From 1a – e the hydrazones 2a – e were prepared as precursors of the corresponding carbenes 4.