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The application of 1H13C inversely correlated NMR spectroscopy to the determination of acylation and glycosylation sites in the O-specific polysaccharide from Hafnia alvei 1187

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Dabrowski,  Janusz
Department of Organic Chemistry, Max Planck Institute for Medical Research, Max Planck Society;

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Hauck,  Michael
Department of Organic Chemistry, Max Planck Institute for Medical Research, Max Planck Society;

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Citation

Dabrowski, J., Hauck, M., Romanowska, E., & Gamian, A. (1987). The application of 1H13C inversely correlated NMR spectroscopy to the determination of acylation and glycosylation sites in the O-specific polysaccharide from Hafnia alvei 1187. Biochemical and Biophysical Research Communications (Orlando, FL), 146(3), 1283-1285. doi:10.1016/0006-291X(87)90787-X.


Cite as: http://hdl.handle.net/21.11116/0000-0007-2C08-0
Abstract
An inversely correlated NMR spectrum defined the amino sugars acylated by acetyl or 3-hydroxybutyryl groups and revealed partial sequences and glycosylation sites in a tetrasacchride repeating unit of the title polysaccharide, (→2dGlcαl→3dGlcNAcylαl→→4dGalNAcαl→3dGalNAcβl→)n, where Acyl = 3-hydroxybutyryl.