Gas-and liquid chromatographic separation of naphthalenophanes of the [2.2] and 
[3.3] type

Deege, A.; Heinecke, B.; Schomburg, G.

doi:10.1007/BF02290435

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Gas-and liquid chromatographic separation of naphthalenophanes of the [2.2] and [3.3] type

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Deege, A.
Service Department Schomburg (GC), Max-Planck-Institut für Kohlenforschung, Max Planck Society;

Heinecke, B.
Service Department Schomburg (GC), Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Schomburg, G.
Service Department Schomburg (GC), Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Citation

Deege, A., Heinecke, B., & Schomburg, G. (1982). Gas-and liquid chromatographic separation of naphthalenophanes of the [2.2] and [3.3] type. Chromatographia, 15(2), 65-70. doi:10.1007/BF02290435.

Cite as: https://hdl.handle.net/21.11116/0000-000A-7656-1

Abstract

Separations of various isomeric naphthalenophanes have been performed in different LC-systems, including those
containing Ag⁺ in the mobile phase, and also by high temperature capillary GC. Ag⁺-complexation in the mobile phase of LC-systems can be observed with several
of the strained aromatic systems, but most of the separations of practical interest can also be achieved without
Ag⁺-complexation. For solubility reasons purification
and isolation of certain isomeric species have been performed in normal phase LC-systems only.