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Journal Article

Online Monitoring of Microscale Liquid-Phase Catalysis Using in-Fiber Raman Spectroscopy

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Schorn,  Florian
International Max Planck Research School, Max Planck Institute for the Science of Light, Max Planck Society;
University of Erlangen-Nürnberg, Dept Phys;
‎Interdisciplinary Ctr Nanostruct Films;
Joly Research Group, Research Groups, Max Planck Institute for the Science of Light, Max Planck Society;

/persons/resource/persons201100

Joly,  Nicolas Y.
Joly Research Group, Research Groups, Max Planck Institute for the Science of Light, Max Planck Society;
University of Erlangen-Nürnberg, Dept Phys;
‎Interdisciplinary Ctr Nanostruct Films;

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Citation

Schorn, F., Aubermann, M., Zeltner, R., Haumann, M., & Joly, N. Y. (2021). Online Monitoring of Microscale Liquid-Phase Catalysis Using in-Fiber Raman Spectroscopy. ACS Catalysis, 11(11), 6709-6714. doi:10.1021/acscatal.1c01264.


Cite as: https://hdl.handle.net/21.11116/0000-0008-D9CA-0
Abstract
We report on the use of hollow-core photonic crystal fibers to monitor the evolution of chemical reactions. The combination of tight confinement and long interaction length allows single-pass spectroscopic measurements using less than a microliter volume of chemicals with good accuracy. As a proof of principle, we used here nonlinear Raman spectroscopy for a reaction screening of the acidic catalyzed esterification of methanol and acetic acid.