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Facile synthesis of novel, known, and low-valent transition metal phosphates via reductive phosphatization

MPS-Authors
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Stegmann,  Niklas
Research Group Schmidt, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Petersen,  Hilke
Research Group Weidenthaler, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Weidenthaler,  Claudia
Research Group Weidenthaler, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Schmidt,  Wolfgang
Research Group Schmidt, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Citation

Stegmann, N., Petersen, H., Weidenthaler, C., & Schmidt, W. (2021). Facile synthesis of novel, known, and low-valent transition metal phosphates via reductive phosphatization. Journal of Materials Chemistry A, 9(34), 18247-18250. doi:10.1039/D1TA03782J.


Cite as: http://hdl.handle.net/21.11116/0000-0009-0B98-0
Abstract
Novel and known low valent transition metal phosphates (TMPs) are accessible via a novel and facile pathway. The method allows syntheses of TMPs also with reduced oxidation states. The key feature of the new route is the reductive character of a hypophosphite salt melt, which acts as reaction medium and enables directing the oxidation state of the transition metal.