Two-dimensional confinement for generating thin single crystals for 
applications in time-resolved electron diffraction and spectroscopy: an 
intramolecular proton transfer study

Hwang, H.; Tiwari, V.; Duan, H.-G.; Bittmann, S.; Tellkamp, F.; Jha, A.; Miller, R. J. D.

doi:10.1039/D2CC02468C

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Journal Article

Two-dimensional confinement for generating thin single crystals for applications in time-resolved electron diffraction and spectroscopy: an intramolecular proton transfer study

MPS-Authors

Hwang, H.
Department of Chemistry, University of Hamburg;
Miller Group, Atomically Resolved Dynamics Department, Max Planck Institute for the Structure and Dynamics of Matter, Max Planck Society;

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Bittmann, S.
Miller Group, Atomically Resolved Dynamics Department, Max Planck Institute for the Structure and Dynamics of Matter, Max Planck Society;
International Max Planck Research School for Ultrafast Imaging & Structural Dynamics (IMPRS-UFAST), Max Planck Institute for the Structure and Dynamics of Matter, Max Planck Society;

Tellkamp, F.
Machine Physics, Scientific Service Units, Max Planck Institute for the Structure and Dynamics of Matter, Max Planck Society;

External Resource

https://doi.org/10.1039/D2CC02468C
(Publisher version)

https://doi.org/10.26434/chemrxiv-2022-w7tlg
(Preprint)

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two-dimensional-confinement-for-generating-thin-single-crystals-for-time-resolved-electron-diffraction-and-spectroscopy-an-intramolecular-proton-transfer-study.pdf
(Preprint), 3MB

Supplementary Material (public)

d2cc02468c1.pdf
(Supplementary material), 3MB

Citation

Hwang, H., Tiwari, V., Duan, H.-G., Bittmann, S., Tellkamp, F., Jha, A., et al. (2022). Two-dimensional confinement for generating thin single crystals for applications in time-resolved electron diffraction and spectroscopy: an intramolecular proton transfer study. Chemical Communications, 58(70), 9774-9777. doi:10.1039/D2CC02468C.

Cite as: https://hdl.handle.net/21.11116/0000-000A-ECC8-B

Abstract

Thin single organic crystals (≤1 μm) with large area (≥100 × 100 μm²) are desirable to explore photoinduced processes using ultrafast spectroscopy and electron-diffraction. Here, we present a general method based on spatial confinement to grow such crystals using the prototypical proton transfer system, 1,5-dihydroxyanthraquinone, as an example, and provide the protocol for optically characterizing structural dynamics to enable proper assignments using diffraction methods.