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Journal Article

Diethyl ether-trichloroborane, (C2H5)2O-BCl3

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Weinmann,  M.
Abteilung Jansen, Former Departments, Max Planck Institute for Solid State Research, Max Planck Society;

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Jansen,  M.
Abteilung Jansen, Former Departments, Max Planck Institute for Solid State Research, Max Planck Society;

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Citation

Weinmann, M., Nuss, J. R., & Jansen, M. (2006). Diethyl ether-trichloroborane, (C2H5)2O-BCl3. Acta Crystallographica E, 62, O5590-O5591.


Cite as: https://hdl.handle.net/21.11116/0000-000E-FEAE-1
Abstract
The title compound, C4H10BCl3O, is the first crystallographically
characterized example of a trihaloborane complex with an ether as
electron-pair donor. The B atom is coordinated tetrahedrally, whereas
oxygen has a strongly distorted coordination environment. The central
B-O bond length is 1.543 (2) angstrom and is thus longer than those in
tetraalkoxyborates, B(OR)(4)(-) .