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Journal Article

Flux-growth and characterization of NaCu2O2 single crystals

MPS-Authors
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Maljuk,  A.
Scientific Facility Crystal Growth (Masahiko Isobe), Max Planck Institute for Solid State Research, Max Planck Society;

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Kulakov,  A. B.
Scientific Facility Crystal Growth (Masahiko Isobe), Max Planck Institute for Solid State Research, Max Planck Society;

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Sofin,  M.
Abteilung Jansen, Former Departments, Max Planck Institute for Solid State Research, Max Planck Society;

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Capogna,  L.
Department Solid State Spectroscopy (Bernhard Keimer), Max Planck Institute for Solid State Research, Max Planck Society;

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Strempfer,  J.
Department Solid State Spectroscopy (Bernhard Keimer), Max Planck Institute for Solid State Research, Max Planck Society;

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Lin,  C. T.
Scientific Facility Crystal Growth (Masahiko Isobe), Max Planck Institute for Solid State Research, Max Planck Society;

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Jansen,  M.
Abteilung Jansen, Former Departments, Max Planck Institute for Solid State Research, Max Planck Society;

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Keimer,  B.
Department Solid State Spectroscopy (Bernhard Keimer), Max Planck Institute for Solid State Research, Max Planck Society;

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Citation

Maljuk, A., Kulakov, A. B., Sofin, M., Capogna, L., Strempfer, J., Lin, C. T., et al. (2004). Flux-growth and characterization of NaCu2O2 single crystals. Journal of Crystal Growth, 263(1-4), 338-343.


Cite as: https://hdl.handle.net/21.11116/0000-000E-FE7A-C
Abstract
For the first time NaCu2O2 single crystals were prepared by a self-flux
technique in Pt crucibles. The as-grown crystals have typical
dimensions of 7 x 3 x 0.1 mm(3). Powder and single crystal XRD
measurements confirm the high quality of the prepared crystals. All
crystals have the orthorhombic structure: a = 6.2087(1) Angstrom, b =
2.9343(1) Angstrom and c = 13.0648(3) Angstrom. DTA-TG and
high-temperature optical microscopy studies show that the NaCu2O2
compound is stable in the temperature range 25-760degreesC and melts
incongruently at 905+/-5degreesC in argon atmosphere. Magnetic
susceptibility measurements carried out on the single crystals showed
clear evidence of antiferromagnetism at T-N = 12.25 K. (C) 2003
Elsevier B.V. All rights reserved.