An Old Story in New Light: X-Ray Powder Diffraction Provides Novel Insights 
into a Long-Known Organic Solid-State Rearrangement Reaction

Halasz, I.; Cindro, N.; Dinnebier, R. E.; Vancik, H.

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An Old Story in New Light: X-Ray Powder Diffraction Provides Novel Insights into a Long-Known Organic Solid-State Rearrangement Reaction

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Dinnebier, R. E.
Scientific Facility X-Ray Diffraction (Robert E. Dinnebier), Max Planck Institute for Solid State Research, Max Planck Society;

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Citation

Halasz, I., Cindro, N., Dinnebier, R. E., & Vancik, H. (2013). An Old Story in New Light: X-Ray Powder Diffraction Provides Novel Insights into a Long-Known Organic Solid-State Rearrangement Reaction. Croatica Chemica Acta, 86(2), 187-192.

Cite as: https://hdl.handle.net/21.11116/0000-000E-C63D-F

Abstract

The first in situ diffraction study of the long-known solid-state rearrangement of p-bromo-benzeneazotribenzoylmethane is reported. This proof-of-principle study demonstrates how modem laboratory X-ray powder diffraction, accompanied by up-to-date processing tools, can be used to monitor and describe mechanisms of organic solid-state reactions while it also underpins its necessity for structural characterisation of in situ formed crystalline phases.