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Journal Article

Synthesis, Separation and Structure Elucidation of a Missing C60 Chloride: C2ν-C60Cl8

MPS-Authors
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Ziegler,  K.
Abteilung Jansen, Former Departments, Max Planck Institute for Solid State Research, Max Planck Society;

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Amsharov,  K. Y.
Department Nanoscale Science (Klaus Kern), Max Planck Institute for Solid State Research, Max Planck Society;
Department Quantum Materials (Hidenori Takagi), Max Planck Institute for Solid State Research, Max Planck Society;

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Jansen,  M.
Abteilung Jansen, Former Departments, Max Planck Institute for Solid State Research, Max Planck Society;

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Citation

Ziegler, K., Amsharov, K. Y., & Jansen, M. (2012). Synthesis, Separation and Structure Elucidation of a Missing C60 Chloride: C2ν-C60Cl8. Zeitschrift für Naturforschung B, 67(10), 1091-1097.


Cite as: https://hdl.handle.net/21.11116/0000-000E-C25C-0
Abstract
The so far missing chloro analog of the bromofullerene C-2v-C60Br8 has been synthesized by reaction of C-60 fullerene with iodine monochloride. The title compound has been separated by means of HPLC, and its molecular structure has been unambiguously determined by single-crystal X-ray analysis. A facile synthesis of C-s-C60Cl6 and C-2v-C60Cl8 in preparative amounts is presented.