A solid-state trimerisation of a diene diacid affords a bicyclobutyl: reactant 
structure from X-ray powder data and product separation and structure 
determination via co-crystallisation

Atkinson, M. B. J.; Halasz, I.; Bucar, D. K.; Dinnebier, R. E.; Mariappan, S. V. S.; Sokolov, A. N.; MacGillivray, L. R.

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A solid-state trimerisation of a diene diacid affords a bicyclobutyl: reactant structure from X-ray powder data and product separation and structure determination via co-crystallisation

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Dinnebier, R. E.
Scientific Facility X-Ray Diffraction (Robert E. Dinnebier), Max Planck Institute for Solid State Research, Max Planck Society;

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Citation

Atkinson, M. B. J., Halasz, I., Bucar, D. K., Dinnebier, R. E., Mariappan, S. V. S., Sokolov, A. N., et al. (2011). A solid-state trimerisation of a diene diacid affords a bicyclobutyl: reactant structure from X-ray powder data and product separation and structure determination via co-crystallisation. Chemical Communications, 47(1), 236-238.

Cite as: https://hdl.handle.net/21.11116/0000-000E-C0E7-4

Abstract

A bicyclobutyl that bears six carboxylic acid groups results from a trimerisation of a diene diacid in the solid state. Powder X-ray diffraction and a co-crystallisation are used to solve the structure of the diene and elucidate the stereochemistry of the bicyclobutyl, respectively.