Electrochemical synthesis of Ag5Pb2O6

Oberndorfer, C. P. M.; Jansen, M.

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Electrochemical synthesis of Ag₅Pb₂O₆

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Oberndorfer, C. P. M.
Abteilung Jansen, Former Departments, Max Planck Institute for Solid State Research, Max Planck Society;

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Jansen, M.
Abteilung Jansen, Former Departments, Max Planck Institute for Solid State Research, Max Planck Society;

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Citation

Oberndorfer, C. P. M., & Jansen, M. (2007). Electrochemical synthesis of Ag₅Pb₂O₆. Zeitschrift für anorganische und allgemeine Chemie, 633(1), 172-175.

Cite as: https://hdl.handle.net/21.11116/0000-000E-B723-C

Abstract

Ag5Pb2O6 was prepared by anodic oxidation of silver in a PbO2 suspension in an aqueous KOH solution. Phase purity was checked by a Rietveld-fit of the X-ray powder pattern, thermal and chemical analysis. The compound exhibits ionic conductivity. It's anisotropy leads to an orientation of the crystallites on the silver anode.